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IQ4 Lesson 12 of 23 50 min Key Reactions

Reactions of Alcohols

Alcohols sit at the crossroads of organic chemistry — they can be converted to alkenes, haloalkanes, aldehydes, ketones, and carboxylic acids, each by changing one reagent or one condition, making them the most synthetically versatile functional group in Module 7.

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Think First — Before You Read

Three Industries, One Molecule

A forensic breathalyser works by oxidising ethanol in breath to ethanoic acid using potassium dichromate — the orange dichromate turns green as it is reduced. A winemaker monitors the souring of wine into vinegar (ethanol → ethanoic acid) when wine is exposed to air. A polymer chemist dehydrates ethanol to ethene, which is then polymerised to polyethylene.

Before you read on: Write down what you think is the structural difference between the product of oxidation (ethanoic acid, CH₃COOH) and the product of dehydration (ethene, CH₂=CH₂). What bonds have been added to, or removed from, the ethanol molecule in each case?

Key Equations — Reactions of Alcohols
Dehydration (Elimination)
R–CH₂–CH₂OH → R–CH=CH₂ + H₂O
conc. H₂SO₄ or conc. H₃PO₄ · heat (~170°C) · atmospheric pressure
Substitution with HX
R–OH + HX → R–X + H₂O
HCl, HBr, or HI · heat under reflux · reactivity: HI > HBr > HCl
Oxidation: 1° → Aldehyde
R–CH₂OH + [O] → R–CHO + H₂O
K₂Cr₂O₇/H⁺ · distillation · orange → green
Oxidation: 1° → Carboxylic Acid
R–CH₂OH + 2[O] → R–COOH + H₂O
excess K₂Cr₂O₇/H⁺ · reflux · orange → green
Oxidation: 2° → Ketone
R–CHOH–R' + [O] → R–CO–R' + H₂O
K₂Cr₂O₇/H⁺ · reflux · orange → green · cannot oxidise further
Tertiary → No Reaction
R–C(OH)(R')(R'') + [O] → no reaction
K₂Cr₂O₇/H⁺ stays ORANGE · no H on C–OH carbon
Learning Intentions
📖

Know

  • Three reactions of alcohols: dehydration, substitution with HX, oxidation
  • Oxidation outcomes: 1° → aldehyde (distillation) or COOH (reflux) · 2° → ketone · 3° → no reaction
  • Colour changes: K₂Cr₂O₇/H⁺ orange→green (oxidation occurred) or stays orange (no oxidation)
  • HX reactivity order: HI > HBr > HCl
💡

Understand

  • Why tertiary alcohols cannot be oxidised — no H on C–OH carbon
  • Why distillation gives aldehyde but reflux gives carboxylic acid from the same primary alcohol
  • Why concentrated (not dilute) acid drives dehydration
  • Why H₂O is always a product of alcohol substitution with HX
✏️

Can Do

  • Write balanced equations for all three reaction types with correct conditions
  • Classify an unknown alcohol as 1°/2°/3° from oxidation test results
  • Select conditions to produce a specific oxidation product from a primary alcohol
  • Construct multi-step synthesis routes using alcohols as intermediates
Key Terms — scan these before reading
DehydrationThe exact reverse of hydration — water is eliminated across the C–OH bond and an adjacent C–H bond, regenerating the C=C.
HydrocarbonAn organic compound containing only carbon and hydrogen atoms.
Functional groupA specific atom arrangement determining characteristic chemical reactions.
Homologous seriesA family of compounds with the same functional group, differing by CH₂.
Addition polymerA polymer formed by monomers adding together without loss of atoms.
Condensation polymerA polymer formed with elimination of a small molecule such as water.
01

Dehydration of Alcohols — Making Alkenes

Dehydration is the exact reverse of hydration — water is eliminated across the C–OH bond and an adjacent C–H bond, regenerating the C=C double bond — and the conditions that drive this reversal are the opposite of those that drive hydration.

Dehydration is an elimination reaction in which an alcohol loses a water molecule (H from one carbon, OH from the adjacent carbon) to form an alkene. It is the reverse of alkene hydration (L06, L10).

R–CH₂–CH₂OH → R–CH=CH₂ + H₂O

Worked Equations

Ethanol → ethene:
CH₃CH₂OH → CH₂=CH₂ + H₂O
Conditions: conc. H₂SO₄, ~170°C

Propan-1-ol → propene:
CH₃CH₂CH₂OH → CH₃CH=CH₂ + H₂O
Conditions: conc. H₂SO₄ or conc. H₃PO₄, heat

Secondary and Tertiary Alcohols — Two Possible Products

When a secondary or tertiary alcohol is dehydrated, the H can be removed from either adjacent carbon, giving two possible alkene products. The major product is the more substituted alkene (more alkyl groups on the C=C carbons). For HSC, NESA accepts any alkene product, but the more substituted alkene is preferred.

Butan-2-ol dehydration:

CH₃CHOHCH₂CH₃ → CH₃CH=CHCH₃ + H₂O  (but-2-ene — major, more substituted)
CH₃CHOHCH₂CH₃ → CH₂=CHCH₂CH₃ + H₂O  (but-1-ene — minor, less substituted)

butan-2-ol (reactant) CH₃ C H OH C H H CH₃ OH + H → H₂O (eliminated) conc. H₂SO₄ heat but-2-ene (major product) CH₃ CH CH CH₃ + H₂O C=C

Dehydration of butan-2-ol — H removed from C3 and OH removed from C2 combine to form H₂O; C=C forms between C2 and C3 giving but-2-ene (major, more substituted product)

Hydration vs. Dehydration — Opposite Conditions

HYDRATION (alkene → alcohol)
dilute acid · high P · high T
adds H₂O across C=C
DEHYDRATION (alcohol → alkene)
conc. acid · atmospheric P · heat
removes H₂O from C–OH and adjacent C–H

Conditions — Dehydration

Reagent
conc. H₂SO₄ or conc. H₃PO₄ (acid catalyst + dehydrating agent)
Temperature
~170°C for ethanol; ~230°C+ for higher alcohols
Pressure
Atmospheric
Equipment
Distillation — removes volatile alkene product as formed
Arrow
→ (elimination; water driven off)
Must Do: The acid in dehydration is CONCENTRATED — not dilute. Dilute acid + high pressure drives hydration (the reverse reaction). Writing "dilute H₂SO₄" for dehydration is wrong — concentrated acid at higher temperature drives dehydration. The concentration of the acid determines the reaction direction.
Common Error: Writing "water is added in dehydration." This is the exact opposite. DEhydration means removing water (–de = removal, hydration = water). The –OH from the alcohol and an H from the adjacent carbon leave together as H₂O — the molecule gets smaller. If water appears as a reactant in your dehydration equation, you have written a hydration reaction instead.
Exam TipFor organic chemistry questions, draw full structural formulas showing all atoms and bonds — condensed or skeletal formulas alone may lose marks in HSC extended-response questions.
02

Substitution of Alcohols with HX — Making Haloalkanes

The reverse of the haloalkane substitution from L10 — instead of converting a haloalkane to an alcohol with NaOH, you can convert an alcohol to a haloalkane with HX — and the conditions and halide reactivity order are what HSC specifically tests.

When an alcohol is treated with a hydrogen halide (HX), the –OH group is replaced by the halogen, producing a haloalkane and water:

R–OH + HX → R–X + H₂O

Worked Equations

CH₃CH₂Br + H₂O  (bromoethane)
Column B

Halide Reactivity Order

HI
fastest
C–I easiest to form
>
HBr
intermediate
>
HCl
slowest
C–Cl hardest to form

Comparison — reverse reactions:

R–OH + HX → R–X + H₂O   (alcohol → haloalkane — this lesson)
R–X + NaOH(aq) → R–OH + NaX   (haloalkane → alcohol — L10)

These are reverse reactions — HX pushes toward haloalkane; NaOH(aq) pushes toward alcohol.

Conditions — Substitution of Alcohol with HX

Reagent
HCl, HBr, or HI (gas or concentrated aqueous solution)
Catalyst
None (ZnCl₂ sometimes used with HCl for primary alcohols)
Conditions
Heat under reflux
Equipment
Reflux condenser; fume cupboard (HX gases are corrosive)
Arrow
→ (substitution; goes essentially to completion)
Must Do: Always include H₂O as a product. R–OH + HBr → R–Br is incomplete — the equation is unbalanced without H₂O. Check: the –OH from the alcohol and the H from HX combine on the right side to give H₂O. Left side: O (from –OH) + H (from HX) = right side: H₂O ✓. Missing H₂O is one of the most commonly penalised equation errors.
Common Error: Confusing R–OH + HX → R–X + H₂O (alcohol substitution) with alkene + HX → haloalkane (hydrohalogenation from L06, addition). Both use HX and produce haloalkanes. The key differences: (1) starting material (alcohol vs alkene); (2) whether H₂O is also produced (yes for alcohol substitution; no for addition); (3) reaction type (substitution vs addition). The presence of H₂O as a product instantly identifies alcohol substitution.
03

Oxidation of Alcohols — The Classification-Dependent Reaction

Oxidation of alcohols is the single most important reaction for understanding how the organic functional group classes connect — primary alcohols become aldehydes and then carboxylic acids, secondary alcohols become ketones, and tertiary alcohols refuse to react — and the reason is structural, not arbitrary.

Why Oxidation Depends on Alcohol Classification

Oxidation of an alcohol involves removing two hydrogen atoms — one H from the C–OH carbon and one H from the –OH oxygen — to form the C=O (carbonyl) bond. For this to be possible, the C–OH carbon must have at least one H atom available to be removed.

C–OH has 2 H atoms → gives aldehyde (distillation) → can further oxidise to carboxylic acid (reflux)
C–OH has 1 H atom → gives ketone. Ketone C=O is flanked by two carbons — no H on carbonyl carbon → cannot be further oxidised
C–OH has 0 H atoms (bonded to 3 carbons) → no H to remove → NO REACTION with K₂Cr₂O₇/H⁺

Oxidising Agents and Colour Changes

K₂Cr₂O₇/H⁺ (acidified dichromate)
Orange (Cr₂O₇²⁻) Green (Cr³⁺)

Colour change = oxidation occurred (1° or 2° alcohol)
No change (stays orange) = no oxidation (3° or no alcohol)

KMnO₄/H⁺ (acidified permanganate)
Purple (MnO₄⁻) Colourless (Mn²⁺)

Under acidic conditions. Colour change = oxidation occurred
(Note: neutral/basic → brown MnO₂ precipitate instead)

Controlling Product from Primary Alcohols — Distillation vs. Reflux

The product from oxidising a primary alcohol depends entirely on the equipment used:

Distillation → Aldehyde

Aldehyde has lower BP than alcohol — collected as it forms before excess oxidant can oxidise it further. Removes product from reaction mixture immediately.

R–CH₂OH + [O] → R–CHO + H₂O
Reflux → Carboxylic Acid

All components stay in flask; excess oxidant has maximum contact time to fully oxidise aldehyde intermediate through to carboxylic acid.

R–CH₂OH + 2[O] → R–COOH + H₂O

Oxidation Summary Table

Alcohol Class Oxidant Equipment Product Colour Change (K₂Cr₂O₇)
Primary (1°)K₂Cr₂O₇/H⁺DistillationAldehydeOrangeGreen
Primary (1°)K₂Cr₂O₇/H⁺ (excess)RefluxCarboxylic acidOrangeGreen
Secondary (2°)K₂Cr₂O₇/H⁺RefluxKetoneOrangeGreen
Tertiary (3°)K₂Cr₂O₇/H⁺AnyNo reactionStays orange
Must Do — Two Conditions Required: For any alcohol oxidation answer, always state: (1) the oxidising agent (K₂Cr₂O₇/H⁺ or KMnO₄/H⁺ — always acidified); AND (2) the equipment (distillation for aldehyde; reflux for carboxylic acid or ketone). Stating only the reagent without the equipment — or vice versa — earns partial marks. The equipment choice determines the product.
Common Error: "Tertiary alcohols give a ketone with KMnO₄." Tertiary alcohols do NOT undergo oxidation with K₂Cr₂O₇/H⁺ or KMnO₄/H⁺ — the solution stays orange (no reduction of Cr₂O₇²⁻ occurs). This is the diagnostic test for tertiary alcohols: K₂Cr₂O₇/H⁺ stays orange → tertiary alcohol (or no alcohol present).
Common Error: "KMnO₄ goes purple → orange." KMnO₄ goes purple → colourless (or very pale pink) when MnO₄⁻ is reduced to Mn²⁺ in acidic solution. It goes purple → brown precipitate (MnO₂) under neutral/alkaline conditions. KMnO₄ NEVER turns orange — orange is the colour of dichromate (K₂Cr₂O₇). Confusing these colour changes is heavily penalised.
04

Alcohols at the Centre — The Reaction Map Hub

Putting dehydration, substitution, and oxidation together with the production reactions from L10 reveals that alcohols are the central hub of the organic reaction map — every arrow into and out of alcohol connects to a different functional group class.

ALCOHOL R–OH ALKENE hydration (L10) HALOALKANE NaOH(aq) (L10) GLUCOSE fermentation (L10) ALKENE conc. H₂SO₄, heat dehydration HALOALKANE + HX, reflux ALDEHYDE (1° only) K₂Cr₂O₇/H⁺ distillation · 1° CARBOXYLIC ACID (1° only) excess K₂Cr₂O₇/H⁺ reflux · 1° KETONE (2° only) K₂Cr₂O₇/H⁺ reflux · 2° NO REACTION (3° stays orange) ARROWS IN (production) ARROWS OUT (this lesson)

Alcohol reaction hub — dashed arrows show production routes (L10); solid arrows show this lesson's reactions. Alcohol is the central node connecting every major functional group class.

Using Colour Changes as Diagnostic Tests

Conclusion
Column B
Must Do: The orange→green colour change confirms oxidation occurred — it does NOT identify the specific product. To determine the product, you need: (1) the conditions (distillation vs. reflux); AND (2) a secondary test on the product (Tollens' for aldehyde vs. litmus for acid). Never write "the product is an aldehyde because the dichromate went green" — the colour change identifies the class (primary/secondary) but not the specific carbonyl product.

⚠️ Common Misconceptions — Reactions of Alcohols

"Dehydration adds water to the alcohol." Dehydration REMOVES water — the prefix "de-" means removal. The –OH and a neighbouring H leave together as H₂O. If water appears as a reactant in your equation, you have written a hydration reaction (the reverse process).

"Tertiary alcohols give ketones when oxidised." Tertiary alcohols do NOT react with K₂Cr₂O₇/H⁺ or KMnO₄/H⁺ — the solution stays orange (or purple). The absence of colour change IS the result for a tertiary alcohol. Only secondary alcohols give ketones on oxidation.

"KMnO₄ turns orange when it oxidises an alcohol." Orange is the colour of dichromate (Cr₂O₇²⁻). Permanganate (MnO₄⁻) is purple and becomes colourless (Mn²⁺) in acidic conditions, or forms a brown precipitate (MnO₂) in neutral/alkaline conditions. KMnO₄ never turns orange.

"You can get either aldehyde or carboxylic acid from a primary alcohol just by changing the oxidant." The key variable is the equipment — distillation vs. reflux — not just the oxidant choice. Reflux with any strong oxidant gives acid; distillation removes the aldehyde before it can be further oxidised regardless of which oxidant is used.

Example 1 Straightforward

Predicting Products of Alcohol Reactions

Problem: For each reaction below, write the balanced equation, name the product, and state all conditions: (a) dehydration of propan-1-ol; (b) reaction of butan-1-ol with HBr; (c) oxidation of propan-2-ol to its maximum oxidation product.
1
(a) Dehydration of propan-1-ol:
Propan-1-ol: CH₃CH₂CH₂OH. Remove H from C2 and –OH from C1 → propene + H₂O.
CH₃CH₂CH₂OH → CH₃CH=CH₂ + H₂O
Product: propene (prop-1-ene)
Conditions: conc. H₂SO₄ (or conc. H₃PO₄) · heat (~170–230°C) · distillation to remove alkene product
2
(b) Butan-1-ol + HBr:
Replace –OH at C1 with Br; H₂O is produced.
CH₃CH₂CH₂CH₂OH + HBr → CH₃CH₂CH₂CH₂Br + H₂O
Product: 1-bromobutane
Conditions: HBr · no catalyst · heat under reflux · fume cupboard
3
(c) Oxidation of propan-2-ol (maximum product):
Propan-2-ol: CH₃CHOHCH₃ — secondary alcohol (C–OH bonded to two carbons). Maximum oxidation product of a secondary alcohol = ketone. Ketones cannot be further oxidised.
CH₃CHOHCH₃ + [O] → CH₃COCH₃ + H₂O
Product: propanone
Conditions: K₂Cr₂O₇/H₂SO₄ (or KMnO₄/H₂SO₄) · reflux · Colour change: orange → green
Answer:
(a) CH₃CH₂CH₂OH → CH₃CH=CH₂ + H₂O (propene). Conc. H₂SO₄, heat, distillation.
(b) CH₃CH₂CH₂CH₂OH + HBr → CH₃CH₂CH₂CH₂Br + H₂O (1-bromobutane). HBr, reflux.
(c) CH₃CHOHCH₃ + [O] → CH₃COCH₃ + H₂O (propanone). K₂Cr₂O₇/H₂SO₄, reflux. Orange → green.
Example 2 Intermediate

Identifying Unknown Alcohols Using Oxidation Tests

Problem: Three unlabelled alcohols — P, Q, R — all have molecular formula C₄H₁₀O. When treated with acidified K₂Cr₂O₇: P stays orange. Q turns green; distillation of the product gives a compound that produces a silver mirror with Tollens' reagent. R turns green; the product does NOT give a silver mirror and does NOT turn litmus red. (a) Classify P, Q, R as 1°/2°/3°. (b) Identify each compound. (c) Write the oxidation equation for Q under reflux conditions.
1
(a) Classify:
P: no colour change with K₂Cr₂O₇/H⁺ → no oxidation → tertiary alcohol
Q: orange → green; product gives positive Tollens' (silver mirror) → aldehyde formed → primary alcohol (oxidised under distillation)
R: orange → green; product is neither aldehyde (negative Tollens') nor carboxylic acid (negative litmus) → ketone formed → secondary alcohol
2
(b) Identify structures (all C₄H₁₀O isomers):
P (tertiary, C₄): only one tertiary C₄ alcohol → 2-methylpropan-2-ol ((CH₃)₃COH) ✓
Q (primary, C₄): butan-1-ol (CH₃CH₂CH₂CH₂OH) or 2-methylpropan-1-ol ((CH₃)₂CHCH₂OH) — both are primary. Most common exam assumption: butan-1-ol.
R (secondary, C₄): only one secondary C₄H₁₀O alcohol → butan-2-ol (CH₃CHOHCH₂CH₃) ✓
3
(c) Oxidation of Q (butan-1-ol) under reflux — maximum product:
Primary alcohol + excess oxidant + reflux → carboxylic acid.
CH₃CH₂CH₂CH₂OH + 2[O] → CH₃CH₂CH₂COOH + H₂O
Product: butanoic acid. Conditions: excess K₂Cr₂O₇/H₂SO₄, reflux. Orange → green.
Answer:
(a) P = tertiary; Q = primary; R = secondary.
(b) P = 2-methylpropan-2-ol; Q = butan-1-ol; R = butan-2-ol.
(c) CH₃CH₂CH₂CH₂OH + 2[O] → CH₃CH₂CH₂COOH + H₂O (excess K₂Cr₂O₇/H₂SO₄, reflux). Orange → green.
Example 3 Extended Response

Multi-Step Conversion from Butan-2-ol (8 marks)

Problem: Starting from butan-2-ol only, describe how you would carry out three conversions. For each step, write the equation, state all conditions, and explain why those conditions give that specific product rather than an alternative.
Conversion 1: butan-2-ol → but-2-ene  |  Conversion 2: butan-2-ol → butanone  |  Conversion 3: butan-2-ol → 2-bromobutane
1
Conversion 1 — butan-2-ol → but-2-ene (dehydration):
CH₃CHOHCH₂CH₃ → CH₃CH=CHCH₃ + H₂O (major product — more substituted)
Also possible: CH₂=CHCH₂CH₃ (but-1-ene, minor). NESA accepts either.
Conditions: conc. H₂SO₄ or conc. H₃PO₄ · heat (~170–230°C) · atmospheric pressure · distillation
Why: concentrated acid protonates the –OH, making it a good leaving group; heating drives the elimination; distillation removes the volatile alkene as it forms, shifting equilibrium toward product.
2
Conversion 2 — butan-2-ol → butanone (oxidation):
Butan-2-ol is a SECONDARY alcohol → oxidation gives a ketone. Ketones cannot be further oxidised.
CH₃CHOHCH₂CH₃ + [O] → CH₃COCH₂CH₃ + H₂O
Product: butanone (butan-2-one). Colour change: orange → green.
Conditions: K₂Cr₂O₇/H₂SO₄ (or KMnO₄/H₂SO₄) · reflux
Why reflux (not distillation): reflux keeps reactants in contact for efficient conversion. There is no risk of over-oxidation to carboxylic acid because ketones are resistant to further oxidation — reflux ensures complete conversion without changing the product type.
3
Conversion 3 — butan-2-ol → 2-bromobutane (substitution with HBr):
Replace –OH at C2 with Br; H₂O produced as second product.
CH₃CHOHCH₂CH₃ + HBr → CH₃CHBrCH₂CH₃ + H₂O
Product: 2-bromobutane.
Conditions: HBr (concentrated or gas) · no catalyst · heat under reflux · fume cupboard
Why HBr (not HCl): HBr reacts faster with secondary alcohols than HCl (C–Br bond forms more readily). Why reflux: reaction is slow at room temperature; heating under reflux increases rate while retaining volatile HBr in the reaction mixture.
Answer Summary:
Conv. 1 (→ alkene): CH₃CHOHCH₂CH₃ → CH₃CH=CHCH₃ + H₂O. Conc. H₂SO₄, heat, distillation.
Conv. 2 (→ ketone): CH₃CHOHCH₂CH₃ + [O] → CH₃COCH₂CH₃ + H₂O. K₂Cr₂O₇/H₂SO₄, reflux. Orange → green.
Conv. 3 (→ haloalkane): CH₃CHOHCH₂CH₃ + HBr → CH₃CHBrCH₂CH₃ + H₂O. HBr, reflux.

DEHYDRATION:
R-CH₂-CH₂OH → R-CH=CH₂ + H₂O
Conditions: conc. H₂SO₄ or H₃PO₄ · heat · distillation
Note: concentrated acid (NOT dilute)

SUBSTITUTION WITH HX:
R-OH + HX → R-X + H₂O
Conditions: HCl/HBr/HI · heat under reflux
Reactivity: HI > HBr > HCl
Always write H₂O as second product!

OXIDATION:
1° + K₂Cr₂O₇/H⁺ + distillation → ALDEHYDE (orange→green)
1° + K₂Cr₂O₇/H⁺ (excess) + reflux → CARBOXYLIC ACID (orange→green)
2° + K₂Cr₂O₇/H⁺ + reflux → KETONE (orange→green)
3° + K₂Cr₂O₇/H⁺ → NO REACTION (stays orange)
KMnO₄/H⁺: purple → colourless (NOT orange!)

Activity A

Conditions Grid — Fill the Gaps

For each transformation below, write: the reagent, the conditions (temperature/equipment), and the type of reaction.

  1. Butan-1-ol → but-1-ene
  2. Pentan-1-ol → pentanal
  3. Pentan-1-ol → pentanoic acid
  4. Propan-2-ol → propanone
  5. Ethanol → bromoethane... wait, that would need only one carbon — actually chloroethane: ethanol + HCl
Activity B

Diagnostic Reasoning — What Alcohol Is This?

An unknown alcohol X (molecular formula C₃H₈O) is tested with the following reagents:

  • K₂Cr₂O₇/H₂SO₄ (reflux): solution turns green; product has a sharp vinegar-like smell
  • Dehydration with conc. H₂SO₄: produces propene

Identify alcohol X, write its structural formula, and explain each piece of evidence. Then write the equation for the oxidation of X to its maximum oxidation product.

Question 1. A student adds excess acidified K₂Cr₂O₇ to pentan-1-ol under reflux. What is the organic product and what colour change is observed?

APentanal; orange → green
BPentanoic acid; orange → green
CPentan-1-one; orange stays orange
DPentanoic acid; purple → colourless

Question 2. Which conditions would convert ethanol to ethanal (acetaldehyde) rather than to ethanoic acid?

AExcess K₂Cr₂O₇/H₂SO₄ under reflux
BK₂Cr₂O₇/H₂SO₄, gentle heating, product collected by distillation
CKMnO₄/H₂SO₄ under reflux
DConc. H₂SO₄, 170°C, distillation

Question 3. A student treats 2-methylpropan-2-ol with acidified K₂Cr₂O₇. What does the student observe, and why?

AOrange → green; a ketone is produced because it is a secondary alcohol
BOrange → green; an aldehyde is produced because the –OH is oxidised
CNo colour change; 2-methylpropan-2-ol is a tertiary alcohol with no H on the C–OH carbon and cannot be oxidised under these conditions
DOrange → green; a carboxylic acid is produced because the –OH is converted to –COOH

Question 4. Which conditions would correctly convert butan-1-ol to butanal (and NOT butanoic acid)?

AExcess KMnO₄/H₂SO₄, reflux
BK₂Cr₂O₇/H₂SO₄, reflux
CK₂Cr₂O₇/H₂SO₄, gentle heating, collect product by distillation as it forms
DConc. H₂SO₄, heat — dehydration gives but-1-ene which can be oxidised to butanal

Question 5. A compound with molecular formula C₄H₈O does not give a positive Tollens' test and does not react with acidified K₂Cr₂O₇ (solution stays orange). What is the most likely identity of this compound?

AButan-1-ol (a primary alcohol)
BButan-2-ol (a secondary alcohol)
CButanal (an aldehyde)
DButan-2-one (a ketone)
Revisit Your Initial Thinking

Look back at what you wrote in the Think First section. What has changed? What did you get right? What surprised you?

Short Answer Questions

Question 6 4 marks

Write balanced equations for three reactions of ethanol: (a) dehydration to ethene; (b) reaction with HBr to form a haloalkane; (c) oxidation to ethanoic acid. For each equation, state the reagents and conditions required.

Question 7 5 marks

The same primary alcohol — pentan-1-ol — can be converted to either pentanal or pentanoic acid using K₂Cr₂O₇/H₂SO₄. (a) Write the equation for each transformation. (b) State the specific conditions (including equipment) that produce each product. (c) Explain why using reflux rather than distillation changes the product from aldehyde to carboxylic acid.

Question 8 6 marks

A student performs a two-step synthesis: Step 1 — ethene is reacted with steam to produce ethanol. Step 2 — ethanol is converted to ethanoic acid. For each step, write the balanced equation, state the reagents and conditions, and explain the role of a specific condition in determining the product (including why reflux in step 2 gives acid rather than aldehyde).

Multiple Choice Answers

Q1 — B: Pentanoic acid; orange → green. Pentan-1-ol is a primary alcohol. Excess K₂Cr₂O₇/H⁺ under REFLUX (not distillation) gives maximum oxidation product = carboxylic acid (pentanoic acid). K₂Cr₂O₇ (orange) → Cr³⁺ (green) as oxidant is reduced. A (pentanal) would result from DISTILLATION (removes aldehyde before further oxidation), not reflux. C is wrong — pentan-1-one would require a secondary alcohol, not a primary one. D has wrong colour change — purple→colourless is KMnO₄ in acid, not K₂Cr₂O₇.
Q2 — B: K₂Cr₂O₇/H₂SO₄, gentle heating, distillation. To produce the aldehyde (not the acid) from a primary alcohol, the aldehyde must be removed before excess oxidant can oxidise it further — achieved by DISTILLATION (aldehyde has lower BP than alcohol). A (excess oxidant, reflux) fully oxidises to ethanoic acid. C (KMnO₄, reflux) is too powerful and gives the acid. D (conc. H₂SO₄, 170°C) describes dehydration to ethene — not oxidation.
Q3 — C: No colour change; tertiary alcohol cannot be oxidised. 2-methylpropan-2-ol is a tertiary alcohol — the C–OH carbon is bonded to three other carbons with no H atoms. Oxidation requires removing H from the C–OH carbon — impossible for a tertiary alcohol. K₂Cr₂O₇/H⁺ stays orange = no reduction of Cr₂O₇²⁻ = no oxidation. This orange/no-change result is the diagnostic test for tertiary alcohols.
Q4 — C: K₂Cr₂O₇/H₂SO₄, gentle heating, distillation. To stop at the aldehyde stage, the aldehyde must be removed from the reaction mixture as soon as it forms — before the oxidant can oxidise it further to butanoic acid. Distillation achieves this because butanal has a lower boiling point than butan-1-ol and can be collected as it distils off. A and B both use reflux — reflux keeps aldehyde in contact with oxidant, allowing full oxidation to carboxylic acid. D is dehydration (wrong reaction type entirely).
Q5 — D: Butan-2-one (a ketone). C₄H₈O has one degree of unsaturation (the C=O group). No reaction with K₂Cr₂O₇/H⁺ (stays orange) → no oxidation → not a primary or secondary alcohol and not an aldehyde. No positive Tollens' → not an aldehyde. C₄H₈O with a C=O that is not an aldehyde = ketone. Butan-2-one (CH₃COCH₂CH₃) is the C₄ ketone. A and B are alcohols (C₄H₁₀O, not C₄H₈O). C (butanal) would give positive Tollens'.

Short Answer Sample Answers

Q6 — Three reactions of ethanol (4 marks):
(a) Dehydration: CH₃CH₂OH → CH₂=CH₂ + H₂O [1 mark]. Conditions: conc. H₂SO₄ (or conc. H₃PO₄), heat (~170°C), distillation [1 mark]
(b) Substitution: CH₃CH₂OH + HBr → CH₃CH₂Br + H₂O [1 mark]. Conditions: HBr, heat under reflux [½ mark; 1 mark for including H₂O as product]
(c) Oxidation to acid: CH₃CH₂OH + 2[O] → CH₃COOH + H₂O [1 mark]. Conditions: excess K₂Cr₂O₇/H₂SO₄ (or KMnO₄/H₂SO₄), reflux [1 mark]
Q7 — Pentanal vs pentanoic acid from pentan-1-ol (5 marks):
(a) Equations:
Pentanal: CH₃CH₂CH₂CH₂CH₂OH + [O] → CH₃CH₂CH₂CH₂CHO + H₂O [1 mark]
Pentanoic acid: CH₃CH₂CH₂CH₂CH₂OH + 2[O] → CH₃CH₂CH₂CH₂COOH + H₂O [1 mark]
(b) Conditions:
Pentanal: K₂Cr₂O₇/H₂SO₄, gentle heating, product collected by DISTILLATION [1 mark]
Pentanoic acid: excess K₂Cr₂O₇/H₂SO₄ (or KMnO₄/H₂SO₄), REFLUX [1 mark]
(c) Explanation: Pentanal has a lower boiling point than pentan-1-ol. Under distillation conditions, pentanal boils off and is removed from the reaction mixture as soon as it forms — before excess oxidant can oxidise it further to pentanoic acid. Under reflux, all volatile components (including the aldehyde intermediate) are condensed and returned to the flask, giving the oxidant maximum contact time to oxidise the aldehyde all the way to the carboxylic acid. The equipment choice (distillation vs. reflux) controls whether the aldehyde is removed before or after further oxidation. [1 mark]
Q8 — Two-step synthesis: ethene → ethanol → ethanoic acid (6 marks):
Step 1 — Ethene hydration:
CH₂=CH₂ + H₂O ⇌ CH₃CH₂OH [1 mark for equation with ⇌]
Conditions: H₂O (steam), H₃PO₄ catalyst, ~300°C, ~65 atm [1 mark]
Role of conditions: High pressure is used because the left side has 2 moles of gas and the right has ~0 (ethanol condenses) — by Le Chatelier, high pressure shifts equilibrium right toward ethanol. 300°C is a rate-yield compromise — lower temperature would give higher yield (exothermic forward reaction) but unacceptably slow rate. [1 mark — Le Chatelier application]
Step 2 — Ethanol oxidation to ethanoic acid:
CH₃CH₂OH + 2[O] → CH₃COOH + H₂O [1 mark for equation with 2[O] and correct products]
Conditions: excess K₂Cr₂O₇/H₂SO₄ (or KMnO₄/H₂SO₄), reflux [1 mark]
Role of reflux: Reflux keeps all volatile components (including the aldehyde intermediate, ethanal) in the reaction flask, giving the excess oxidant maximum contact time to oxidise ethanal through to ethanoic acid. If distillation were used instead, ethanal would be removed before further oxidation, and the product would be ethanal (not ethanoic acid). [1 mark]
Revisit — Think First

Three Industries, One Molecule — Structural Analysis

Return to your prediction about the structural difference between ethanoic acid (oxidation) and ethene (dehydration), both starting from ethanol.

Oxidation (ethanol → ethanoic acid): Two H atoms are removed and replaced with a C=O and an OH group. The carbon count stays at 2, the chain stays intact, but the functional group changes from –OH to –COOH. The molecule gains an oxygen (from the oxidising agent). Net: H₂ removed, [O] added.

Dehydration (ethanol → ethene): The –OH group and an H from the adjacent carbon leave together as H₂O. The carbon count stays at 2, the molecule gets smaller (loses H₂O), and a C=C double bond forms where the C–OH and C–H bonds were. Net: H₂O removed, C=C formed.

The breathalyser, the winemaker, and the polymer chemist are each exploiting a different reactivity of the same –OH group: oxidation to –COOH, further oxidation to –COOH, and elimination of –OH as water respectively. One functional group, three industries, three completely different products.

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Speed Race

Reactions of Alcohols — Dehydration, Substitution & Oxidation

Answer questions on Reactions of Alcohols — Dehydration, Substitution & Oxidation before your opponents cross the line. Fast answers = faster car. Pool: lessons 1–12.