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IQ5 Lesson 14 of 23 45 min Carboxylic Acids

Carboxylic Acids

Carboxylic acids are everywhere you can smell or taste sourness — vinegar, citrus fruit, rancid butter, and the lactic acid in sore muscles — and their chemistry connects the physical properties of IMF to the equilibrium chemistry of Module 6 in one of the most integrated lessons in the HSC course.

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Think First — Before You Read

Wine Turns to Vinegar — A 40°C Mystery

Ethanoic acid (acetic acid) and ethanol are both two-carbon compounds with oxygen, and both are found in wine — ethanol as the intended product of fermentation, ethanoic acid as the unwanted product when wine sours on exposure to air. Vinegar is 5% ethanoic acid in water.

Despite having similar molecular masses (ethanol 46 g/mol, ethanoic acid 60 g/mol), ethanoic acid boils at 118°C while ethanol boils at 78°C — a difference of 40°C despite the acid being heavier. Both compounds have an O–H bond and can form hydrogen bonds.

Before you read on: Write down your explanation for why ethanoic acid has such a dramatically higher boiling point than ethanol. What do you think the carboxyl group (–COOH) can do that the hydroxyl group (–OH) cannot? Record your best prediction below.

Key Expressions

General formula
R–COOH  (CnH2nO2)
Carboxyl group = C=O + O–H on same C
Weak acid ionisation
R–COOH + H₂O ⇌ R–COO⁻ + H₃O⁺
Ka = [R–COO⁻][H₃O⁺] / [R–COOH]   Ka ≪ 1
With NaOH
R–COOH + NaOH → R–COONa + H₂O
No gas; salt + water
With Na₂CO₃
2R–COOH + Na₂CO₃ → 2R–COONa + H₂O + CO₂↑
Effervescence (CO₂); salt + water + gas
With NaHCO₃
R–COOH + NaHCO₃ → R–COONa + H₂O + CO₂↑
Key diagnostic — only carboxylic acids do this
With reactive metal
2R–COOH + Mg → (R–COO)₂Mg + H₂↑
H₂ gas; metal salt formed
pKa comparison
Carboxylic acid (~5) < Phenol (~10) < Alcohol (~16)
Lower pKa = stronger acid; carboxylic acid strongest
Esterification (preview L15)
R–COOH + R'OH ⇌ R–COOR' + H₂O
Conc. H₂SO₄ catalyst, heat under reflux
Know
  • The carboxyl group (–COOH) consists of a carbonyl and a hydroxyl on the same carbon
  • General formula of carboxylic acids: CnH2nO2; suffix –oic acid
  • Carboxylic acids form hydrogen-bonded dimers in the liquid phase
  • Carboxylic acids are weak acids (Ka ≪ 1); partially ionise in water
  • Acid strength order: carboxylic acid > phenol > alcohol
Understand
  • Why dimerisation causes carboxylic acids to have higher BPs than alcohols of the same chain length
  • Why the carboxylate anion (R–COO⁻) is more stable than the alkoxide (R–O⁻) due to resonance
  • Why the NaHCO₃ test distinguishes carboxylic acids from phenols and alcohols
  • How short-chain carboxylic acids are fully miscible with water
Can Do
  • Write IUPAC names and structural formulae for C1–C5 carboxylic acids
  • Write balanced equations for all four reactions (NaOH, Na₂CO₃, NaHCO₃, reactive metal)
  • Explain dimerisation and link it to anomalous boiling points
  • Use the NaHCO₃ diagnostic test in an unknown identification question
  • Apply resonance to compare acid strength of carboxylic acid vs alcohol
01

The Carboxyl Group — Structure and Unique Bonding

The carboxyl group (–COOH) is not simply a carbonyl plus a hydroxyl side by side — the two parts interact electronically in ways that give carboxylic acids properties that neither aldehydes, ketones, nor alcohols possess individually.

Structure of the Carboxyl Group

The carboxyl group consists of a carbonyl (C=O) and a hydroxyl (–OH) bonded to the same carbon. That carbon is sp²-hybridised (trigonal planar, ~120° bond angles). The functional group is written –COOH in condensed formulae. In a full structural formula, both oxygens must be drawn explicitly — one with a double bond, one with a single bond to H. The two oxygens are not equivalent.

Two H-Bonding Roles in One Group

Each carboxylic acid molecule can both donate and accept H-bonds:

  • O–H bond → H-bond donor: the O–H hydrogen is δ⁺. The adjacent C=O withdraws electron density, making the O–H bond more polar and the H more acidic than in a simple alcohol.
  • C=O group → H-bond acceptor: lone pairs on the carbonyl oxygen accept H-bonds. (Same as in aldehydes and ketones.)

Dimerisation

Two R–COOH molecules can align face-to-face and form two simultaneous hydrogen bonds in a cyclic, 8-membered ring structure called a dimer:

  • O–H (mol 1) ··· O=C (mol 2)
  • O=C (mol 1) ··· H–O (mol 2)

The dimer is highly stable. In liquid carboxylic acids, a significant proportion of molecules exist as dimers rather than free monomers. Near the boiling point, carboxylic acid vapour density measurements show an effective molecular mass approximately double the monomer mass — confirming molecules predominantly leave the liquid surface as pairs.

H₃C C O δ– O H δ+ CH₃ C O δ– O H δ+ × 2 H-bonds Cyclic dimer — two simultaneous H-bonds; effective mass ≈ 2× monomer

Ethanoic acid hydrogen-bonded dimer. Two carboxyl groups lock together via two simultaneous H-bonds (dashed blue lines, crossing to form the 8-membered ring). Both H-bonds must break to vaporise — this is why carboxylic acid BPs are anomalously high.

IUPAC Naming

Suffix: –oic acid. The –COOH carbon is always C1 (no locant needed). The chain length includes the carbonyl carbon.

CH₃COOH
CH₃CH₂CH₂COOH
Acetic acid (vinegar)
Butyric acid (rancid butter)
Must Do: In any structural formula of a carboxylic acid, draw the –COOH group with both the C=O (two lines from C to O) and the O–H (single bond from the second O to H) explicitly. The two oxygens are not equivalent: one is double-bonded, one carries a hydrogen. Do not write just –CO₂H in a full structural formula — show every bond separately.
Common Error: "Carboxylic acids have two OH groups and therefore form two H-bonds per molecule." The carboxyl group has only ONE O–H bond. The C=O oxygen does NOT have an H — it accepts H-bonds but cannot donate them. Each molecule has exactly one H-bond donor (the O–H) and two acceptor sites (lone pairs on C=O and on the –OH oxygen). In a dimer, each molecule donates one H-bond and accepts one — the result is two H-bonds per dimer pair.
Insight: Methanoic acid (HCOOH) is unique — its "R group" is just H, giving it both –COOH character and an H–C=O component resembling an aldehyde. This means methanoic acid gives a positive Tollens' test (silver mirror) — a property no other simple carboxylic acid has. If you see C₁H₂O₂ give a positive Tollens', it is methanoic acid, not an aldehyde.
Exam TipFor organic chemistry questions, draw full structural formulas showing all atoms and bonds — condensed or skeletal formulas alone may lose marks in HSC extended-response questions.
02

Physical Properties — Why Carboxylic Acids Have Anomalously High Boiling Points

Carboxylic acids consistently have the highest boiling points among organic compounds of comparable chain length — higher than even alcohols — and the explanation is dimerisation, not simply "strong H-bonds."

Boiling Point Trend (same carbon number)

Alkane < Aldehyde ≈ Ketone < Alcohol < Carboxylic acid

Ethane
−89°C
Dispersion only
Ethanal
20°C
Dipole–dipole
Ethanol
78°C
H-bonding (1 per mol)
Ethanoic acid
118°C
Dimer (2 H-bonds/pair)
Key Terms — scan these before reading
HydrocarbonAn organic compound containing only carbon and hydrogen atoms.
Functional groupA specific atom arrangement determining characteristic chemical reactions.
Homologous seriesA family of compounds with the same functional group, differing by CH₂.
Addition polymerA polymer formed by monomers adding together without loss of atoms.
Condensation polymerA polymer formed with elimination of a small molecule such as water.
EsterificationA condensation reaction between a carboxylic acid and an alcohol forming an ester.

Why Carboxylic Acid BP > Alcohol BP (same chain length)

Both ethanoic acid and ethanol have one O–H bond and can form hydrogen bonds. The difference is dimerisation:

  • Two carboxylic acid molecules form a cyclic dimer with two simultaneous H-bonds. To vaporise ethanoic acid, both H-bonds of a dimer must be broken simultaneously.
  • The energy required to disrupt this doubly-bonded pair is significantly greater than the energy to break the single O–H H-bond between two ethanol molecules.
  • The effective unit leaving the liquid surface is the dimer (effective mass ~120 g/mol for ethanoic acid), not the monomer (60 g/mol). This is confirmed by vapour density measurements near the boiling point.

Water Solubility

Short-chain carboxylic acids (C1–C4) are fully miscible with water — the –COOH group forms strong H-bonds with water and the carboxylate anion produced by partial ionisation is fully solvated. From C5 onward, solubility decreases as the non-polar alkyl chain increasingly dominates. Long-chain fatty acids (C12–C22) are essentially insoluble — a property central to biological membranes and soaps (Lesson 17).

Must Do: When explaining why a carboxylic acid has a higher boiling point than an alcohol of the same chain length, you MUST mention dimerisation specifically — not just "stronger H-bonds." The key is that the carboxyl group forms TWO H-bonds per dimer pair simultaneously. Name the dimer, explain its formation, and link it to the higher energy required for vaporisation.
Common Error: "Carboxylic acids have higher boiling points because the –COOH group contains more oxygen atoms." The number of oxygen atoms is not a reliable predictor of boiling point — the type and number of H-bonds formed is what matters. Always reason from IMF type and H-bond quantity, not atom count.
03

Carboxylic Acids as Weak Acids — Reactions and Ka

Carboxylic acids are weak acids — they partially ionise in water rather than fully dissociating — and this equilibrium behaviour, learned in Module 6, now applies directly to predicting which reagents they react with and at what rate.

Weak Acid Ionisation

In water, carboxylic acids establish a partial ionisation equilibrium:

Ionisation equilibrium R–COOH + H₂O ⇌ R–COO⁻ + H₃O⁺
Ka = [R–COO⁻][H₃O⁺] / [R–COOH]  ≪ 1

For ethanoic acid, Ka = 1.8 × 10⁻⁵ (pKa = 4.74). At equilibrium, only ~1% of CH₃COOH molecules are ionised in a 0.1 mol/L solution. Despite being "weak," carboxylic acids are significantly more acidic than alcohols (Ka ~ 10⁻¹⁶) or water.

Why Carboxylic Acids Are Stronger Acids Than Alcohols

After a carboxylic acid donates a proton, the carboxylate anion (R–COO⁻) is stabilised by resonance — the negative charge is delocalised across both oxygens equally. This makes the carboxylate a weaker conjugate base (less tendency to re-accept H⁺), shifting equilibrium further right.

In an alcohol, after proton donation, the alkoxide (R–O⁻) has the negative charge localised on one oxygen — no resonance stabilisation. Stronger base → equilibrium lies far left → much weaker acid.

The Four Reactions

Reaction 1 — With NaOH (neutralisation) CH₃CH₂COOH + NaOH → CH₃CH₂COONa + H₂O
Observable: no gas; pH rises; slightly exothermic; all carboxylic acids react
Reaction 2 — With Na₂CO₃ 2CH₃CH₂COOH + Na₂CO₃ → 2CH₃CH₂COONa + H₂O + CO₂↑
Observable: effervescence (CO₂ bubbles); solid Na₂CO₃ dissolves
Reaction 3 — With NaHCO₃ (KEY DIAGNOSTIC) CH₃CH₂COOH + NaHCO₃ → CH₃CH₂COONa + H₂O + CO₂↑
Observable: effervescence; ONLY carboxylic acids produce CO₂ with NaHCO₃ — phenols and alcohols do NOT
Reaction 4 — With reactive metals (e.g. Mg) 2CH₃CH₂COOH + Mg → (CH₃CH₂COO)₂Mg + H₂↑
Observable: metal dissolves; H₂ gas bubbles; slightly exothermic
Must Do: The reaction with NaHCO₃ that produces CO₂ is the KEY diagnostic test distinguishing carboxylic acids from phenols and alcohols. Carboxylic acids (pKa ~5): react with NaHCO₃ → CO₂. Phenols (pKa ~10): react with NaOH but NOT NaHCO₃. Alcohols (pKa ~16): react with neither. This single test sorts them in one step.
Common Error: Students omit CO₂ from the NaHCO₃ equation. The full product set is carboxylate salt + water + CO₂. The CO₂ arises because HCO₃⁻ accepts the proton → H₂CO₃ → H₂O + CO₂. Without CO₂ your equation is unbalanced — an extra carbon and two extra oxygens are unaccounted for on the right side.
04

Acid Strength Comparison — Carboxylic Acid > Phenol > Alcohol

The acid strength ranking of organic compounds directly reflects the structural stability of their conjugate bases — the more stable the conjugate base, the stronger the acid, and this can be predicted from structure without memorising a list.

The pKa Ranking

Carboxylic acid
pKa ≈ 5 → STRONGEST
Resonance: 2 O atoms share charge
Phenol
pKa ≈ 10 → intermediate
Partial delocalisation into ring
Alcohol
pKa ≈ 16 → weakest
No resonance; charge on 1 O

Structural Basis for the Ranking

Carboxylic acid

R–COO⁻ R–C(=O)–O⁻ ↔ R–C(–O⁻)=O Charge on BOTH oxygens equally — high resonance stabilisation pKa ≈ 5

Phenol

C₆H₅–O⁻ Charge spreads into ring carbons Partial delocalisation — moderate stabilisation pKa ≈ 10

Alcohol

R–O⁻ Charge on ONE oxygen only No resonance — unstabilised, very strong base pKa ≈ 16

The NaHCO₃ / Na₂CO₃ Discrimination Ladder

Compound class NaOH Na₂CO₃ NaHCO₃
Carboxylic acid (pKa ~5) Reacts ✓ CO₂ ✓ CO₂ ✓
Phenol (pKa ~10) Reacts ✓ Reacts ✓ No reaction ✗
Alcohol (pKa ~16) No reaction ✗ No reaction ✗ No reaction ✗
Must Do: Memorise the NaHCO₃/Na₂CO₃ diagnostic matrix above. In extended response identification questions, flow: (1) reacts with NaHCO₃ + CO₂? → carboxylic acid; (2) reacts with Na₂CO₃ but not NaHCO₃? → phenol; (3) reacts with neither? → alcohol. This three-step flowchart handles the most common HSC identification scenarios.
Common Error: "Phenol is a type of alcohol because it has an –OH group." Phenol is NOT an alcohol — the –OH is attached to a benzene ring (aromatic carbon), not an sp³ carbon. This gives phenol fundamentally different properties: more acidic (pKa 10 vs 16), reacts with NaOH readily (alcohols do not under standard conditions), and does not undergo the same oxidation reactions as alcohols. The –OH group alone does not classify a compound as an alcohol.

⚠ Common Misconceptions to Eliminate

"The –COOH group has two O–H bonds." It has ONE O–H bond (the hydroxyl part). The C=O oxygen has no attached hydrogen — it only accepts H-bonds, it cannot donate them.

"Carboxylic acids form stronger individual H-bonds than alcohols." The O–H hydrogen bond type is essentially the same in both. The difference in boiling point comes from dimerisation (two simultaneous H-bonds per pair), not from individual bond strength.

"Carboxylic acids fully ionise in water because they react with NaHCO₃." The reaction with NaHCO₃ reflects acid strength (pKa ~5 vs ~10), not complete ionisation. Carboxylic acids remain weak acids — Ka ≪ 1, only ~1% ionised at typical concentrations.

Example 1 — Writing Equations for Carboxylic Acid Reactions

GIVEN

Propanoic acid (CH₃CH₂COOH). Write balanced equations for reactions with: (a) NaOH, (b) Na₂CO₃, (c) NaHCO₃, (d) Mg.

FIND

Balanced equations and names of products for each reaction.

METHOD

For each reaction, identify the base/metal, apply the general carboxylic acid reaction pattern, and verify atom balance.

STEP 1

(a) With NaOH — acid-base neutralisation; H from –COOH transfers to OH⁻:

CH₃CH₂COOH + NaOH → CH₃CH₂COONa + H₂O
Products: sodium propanoate + water. No gas.
STEP 2

(b) With Na₂CO₃ — two –COOH groups donate H⁺ to CO₃²⁻; forms H₂CO₃ → H₂O + CO₂:

2CH₃CH₂COOH + Na₂CO₃ → 2CH₃CH₂COONa + H₂O + CO₂(g)
Check: Left C = 3×2+1=7; Right C = 3×2+1=7 ✓. Left H = 6×2=12; Right H = 5×2+2=12 ✓
STEP 3

(c) With NaHCO₃ — one –COOH donates H⁺ to HCO₃⁻ → H₂CO₃ → H₂O + CO₂:

CH₃CH₂COOH + NaHCO₃ → CH₃CH₂COONa + H₂O + CO₂(g)
Key diagnostic: only carboxylic acids produce CO₂ with NaHCO₃.
STEP 4

(d) With Mg — two –COOH groups donate H⁺ to Mg; Mg oxidised; H₂ gas produced:

2CH₃CH₂COOH + Mg → (CH₃CH₂COO)₂Mg + H₂(g)
Products: magnesium propanoate (ionic salt) + hydrogen gas. Mg dissolves; bubbles visible.
ANSWER

(a) CH₃CH₂COOH + NaOH → CH₃CH₂COONa + H₂O  |  (b) 2CH₃CH₂COOH + Na₂CO₃ → 2CH₃CH₂COONa + H₂O + CO₂  |  (c) CH₃CH₂COOH + NaHCO₃ → CH₃CH₂COONa + H₂O + CO₂  |  (d) 2CH₃CH₂COOH + Mg → (CH₃CH₂COO)₂Mg + H₂

Example 2 — Explaining Boiling Point and Acid Strength

GIVEN

(a) Ethanoic acid (M = 60 g/mol, BP 118°C) has a significantly higher boiling point than ethanol (M = 46 g/mol, BP 78°C). Explain using IMF reasoning, noting ethanol has a lower molecular mass.  (b) Explain why ethanoic acid is a stronger acid than ethanol using structural reasoning.

STEP 1 — BP comparison

Both ethanoic acid and ethanol have O–H bonds and can form hydrogen bonds. The BP difference (40°C) cannot be explained by molecular mass (acid is heavier) or by one O–H bond alone (each has one O–H).

The key difference is dimerisation. Two ethanoic acid molecules form a cyclic dimer with two simultaneous H-bonds: O–H (mol 1) ··· O=C (mol 2) and O=C (mol 1) ··· H–O (mol 2). To vaporise ethanoic acid, both H-bonds of a dimer must be broken simultaneously — greater energy than breaking the single H-bond between two ethanol molecules. The effective unit leaving the liquid is the dimer (~120 g/mol effective mass).

STEP 2 — Acid strength

Both compounds lose a proton from an O–H bond. The difference is in conjugate base stability:

  • Ethanol → ethoxide (CH₃CH₂O⁻): negative charge localised on one oxygen — no resonance. High-energy anion → very strong base → equilibrium far left → very weak acid (pKa ~16).
  • Ethanoic acid → ethanoate (CH₃COO⁻): negative charge delocalised across both oxygens by resonance: CH₃–C(=O)–O⁻ ↔ CH₃–C(–O⁻)=O. Each oxygen carries ~½ negative charge. Resonance-stabilised anion → weaker base → equilibrium further right → stronger acid (pKa 4.74).
ANSWER

(a) Ethanoic acid forms H-bonded dimers (two simultaneous H-bonds per pair). The effective vaporising unit is the dimer (~120 g/mol), requiring more energy than breaking ethanol's single H-bond → higher BP despite lower monomer mass.  (b) Ethanoate ion is resonance-stabilised (charge on both O equally) → weaker conjugate base → stronger acid (pKa ~5). Ethoxide has charge on one O only — no resonance → stronger base → ethanol is a much weaker acid (pKa ~16).

Example 3 — Identifying an Unknown from Test Results

GIVEN

Unknown compound X has molecular formula C₄H₈O₂. Tests performed:

Stays blue
Column B

(a) Identify the functional group class and explain each test. (b) Write TWO structural isomers of X with IUPAC names. (c) Explain how NaHCO₃ distinguishes a carboxylic acid from an ester (both C₄H₈O₂). (d) Which isomer has the higher boiling point and why?

STEP 1 — Identify class from tests

C₄H₈O₂ fits CₙH₂ₙO₂ — could be a carboxylic acid or an ester (both have two oxygens).

  • Tollens'/Fehling's negative → not an aldehyde ✓
  • NaHCO₃ → effervescence (CO₂) → compound is acidic enough to react with HCO₃⁻. Only carboxylic acids produce CO₂ with NaHCO₃. Esters do not. → X is a carboxylic acid.
  • Br₂ water: no decolourisation → no C=C unsaturation → saturated acid ✓
  • K₂Cr₂O₇ stays orange → carboxylic acids are already at maximum oxidation state for the carboxyl carbon; no further oxidation ✓
STEP 2 — Structural isomers

C₄H₈O₂ carboxylic acid: –COOH group accounts for 1C + 2O. Remaining: 3C, 7H → propyl group (C₃H₇–).

  • Butanoic acid: CH₃CH₂CH₂COOH (straight chain, n-butyric acid)
  • 2-methylpropanoic acid: (CH₃)₂CHCOOH (branched, isobutyric acid)
STEP 3 — NaHCO₃ vs ester

Esters (R–COO–R') have no O–H bond — no acidic hydrogen to donate to HCO₃⁻. The ester linkage (–COO–) does not react with NaHCO₃ under ordinary conditions. Carboxylic acids (pKa ~5) are acidic enough to donate H⁺ to HCO₃⁻, producing H₂CO₃ → H₂O + CO₂ gas (effervescence). The NaHCO₃ test therefore distinguishes: carboxylic acid → CO₂; ester → no reaction.

STEP 4 — Higher BP isomer

Both are carboxylic acids with one –COOH — same H-bonding capability. The difference is dispersion forces: branching in 2-methylpropanoic acid creates a more compact shape → less surface area → weaker dispersion forces. Butanoic acid (straight chain, greater surface area, stronger dispersion) has the higher boiling point (164°C vs 154°C).

ANSWER

(a) X is a saturated carboxylic acid. NaHCO₃ + CO₂ confirms. Tollens'/Fehling's negative rules out aldehyde. No Br₂ decolourisation → saturated. K₂Cr₂O₇ unchanged → already at maximum oxidation state.  (b) Butanoic acid (CH₃CH₂CH₂COOH) and 2-methylpropanoic acid ((CH₃)₂CHCOOH).  (c) Esters lack acidic O–H; carboxylic acids (pKa ~5) donate H⁺ to HCO₃⁻ → CO₂.  (d) Butanoic acid (straight chain, greater surface area, stronger dispersion forces, BP 164°C) > 2-methylpropanoic acid (branched, BP 154°C).

Carboxylic Acids — Summary Notes

Structure: Carboxyl group = –COOH (carbonyl C=O + hydroxyl –OH on same C). General formula: CₙH₂ₙO₂. Suffix: –oic acid; –COOH carbon always C1.

Dimerisation: Two –COOH molecules form a cyclic dimer via two simultaneous H-bonds. To vaporise: both H-bonds must break simultaneously → highest BPs among organic compounds of same chain length (higher than alcohols).

BP trend (same chain length): Alkane < Aldehyde ≈ Ketone < Alcohol < Carboxylic acid

Weak acid: R–COOH + H₂O ⇌ R–COO⁻ + H₃O⁺   Ka ≪ 1. Ethanoic acid Ka = 1.8 × 10⁻⁵.

Reactions:
+ NaOH → salt + H₂O (no gas)
+ Na₂CO₃ → salt + H₂O + CO₂↑
+ NaHCO₃ → salt + H₂O + CO₂↑ (KEY diagnostic)
+ Na/Mg → salt + H₂↑

Acid strength: Carboxylic acid (pKa ~5) > Phenol (~10) > Alcohol (~16). Carboxylate R–COO⁻ is resonance-stabilised (charge on 2 O) → weaker base → stronger acid.

NaHCO₃ test: Carboxylic acid → CO₂; Phenol → no reaction; Alcohol → no reaction.

Activity 1 — Acid Identification Flowchart

Three unknown compounds (P, Q, R) each have molecular formula C₃H₆O₂. The following tests are carried out. Complete the table and identify each compound.

Test P Q R
NaHCO₃ solutionEffervescenceNo reactionNo reaction
Tollens' reagentNo reactionSilver mirrorNo reaction
K₂Cr₂O₇/H⁺Orange → stays orangeOrange → greenOrange → stays orange

Identify P, Q, and R. For each, write the IUPAC name and a short justification (1–2 sentences per compound). Note: C₃H₆O₂ compounds can include carboxylic acids, esters, and aldehydes.

Activity 2 — Boiling Point Prediction and IMF Reasoning

Rank the following five compounds from lowest to highest boiling point. Then explain the position of each compound using IMF reasoning.

  • Propane (C₃H₈)
  • Propanal (C₃H₆O)
  • Propan-1-ol (C₃H₈O)
  • Propanoic acid (C₃H₆O₂)
  • Propanone (C₃H₆O)

Multiple Choice

1. Which of the following correctly describes why ethanoic acid (BP 118°C) has a higher boiling point than ethanol (BP 78°C), despite ethanol having a lower molecular mass?

2. A student adds NaHCO₃ solution to three unlabelled compounds: propanoic acid (P), propan-1-ol (Q), and propyl propanoate (R, an ester). Which observation correctly distinguishes them?

3. Which structural feature of the carboxylate ion (R–COO⁻) makes carboxylic acids stronger acids than alcohols?

4. A compound with molecular formula C₃H₆O₂ produces CO₂ when added to NaHCO₃ solution and gives no reaction with Tollens' reagent. Which compound is it?

5. A 0.1 mol/L solution of ethanoic acid has a pH of approximately 2.9, while a 0.1 mol/L solution of HCl has a pH of 1.0. Which statement best explains this difference?

Short Answer

Question 6 (4 marks) — Butanoic acid (CH₃CH₂CH₂COOH) is the compound responsible for the smell of rancid butter. Write balanced equations for the reactions of butanoic acid with each of the following reagents. Name all products and state one observable for each reaction.

(a) NaOH(aq)  (b) NaHCO₃(aq)  (c) Magnesium metal (Mg)

Question 7 (5 marks) — Explain why propanoic acid (C₂H₅COOH, BP 141°C) has a significantly higher boiling point than propan-1-ol (C₃H₇OH, BP 97°C), given that both have an O–H bond and similar molecular masses (propanoic acid 74 g/mol, propan-1-ol 60 g/mol). In your response, refer to the structure of the carboxylic acid dimer and explain what must occur during vaporisation.

Question 8 (6 marks) — "Carboxylic acids are significantly more acidic than alcohols despite both containing an O–H bond." Using structural arguments, explain this statement by comparing the stability of the carboxylate anion (R–COO⁻) with the alkoxide anion (R–O⁻). Then evaluate the following student claim: "We could increase the acid strength of ethanoic acid by substituting electronegative atoms into the alkyl chain, such as forming chloroethanoic acid (CH₂ClCOOH, pKa 2.86)." Is the student correct? Justify your answer.

Multiple Choice Answers

Q1 — B. Dimerisation is the key. Two ethanoic acid molecules form a cyclic pair with two simultaneous H-bonds; breaking both requires more energy than breaking ethanol's single H-bond. Option A counts O atoms — not valid. Option C confuses intramolecular bond strength with intermolecular forces. Option D confuses viscosity (a consequence) with the cause.

Q2 — A. Only carboxylic acids react with NaHCO₃ to produce CO₂. Propan-1-ol (pKa ~16) is far too weak an acid. Propyl propanoate is an ester — no acidic O–H. The NaHCO₃ test uniquely identifies the carboxylic acid.

Q3 — B. Resonance delocalises the negative charge across both O atoms in R–COO⁻, stabilising it. A more stable conjugate base = weaker base = stronger acid. Option A (more lone pairs) is not a valid stability argument. Option C (size) is a secondary effect, not the primary mechanism at HSC level.

Q4 — B. C₃H₆O₂ with NaHCO₃ → CO₂ means carboxylic acid. Propanoic acid (CH₃CH₂COOH) fits. Methyl ethanoate and ethyl methanoate are esters — no reaction with NaHCO₃. Propanal has formula C₃H₆O (only one oxygen).

Q5 — B. HCl fully dissociates → [H₃O⁺] = 0.1 mol/L → pH 1.0. Ethanoic acid partially ionises (Ka = 1.8 × 10⁻⁵) → only ~1% ionised → [H₃O⁺] ≪ 0.1 mol/L → pH ~2.9. Molecular mass (A) is irrelevant. There is no temperature requirement for the ionisation (C). CH₃ groups do not neutralise H₃O⁺ (D).

Short Answer Sample Answers

Q6 (4 marks):

(a) CH₃CH₂CH₂COOH + NaOH → CH₃CH₂CH₂COONa + H₂O  | Products: sodium butanoate + water  | Observable: no gas produced; pH rises (1 mark)

(b) CH₃CH₂CH₂COOH + NaHCO₃ → CH₃CH₂CH₂COONa + H₂O + CO₂(g)  | Products: sodium butanoate + water + carbon dioxide  | Observable: effervescence/CO₂ bubbles (1 mark)

(c) 2CH₃CH₂CH₂COOH + Mg → (CH₃CH₂CH₂COO)₂Mg + H₂(g)  | Products: magnesium butanoate + hydrogen gas  | Observable: Mg dissolves; H₂ gas bubbles (1 mark); overall balance (1 mark)

Q7 (5 marks) — sample: Both propanoic acid and propan-1-ol possess an O–H bond capable of hydrogen bonding (1 mark). However, propanoic acid molecules form hydrogen-bonded dimers — two molecules align and simultaneously form two H-bonds: O–H (mol 1) ··· O=C (mol 2) and O=C (mol 1) ··· H–O (mol 2), creating a stable cyclic structure (1 mark). To vaporise propanoic acid, both H-bonds of the dimer must be broken simultaneously — the effective unit leaving the liquid is the dimer (effective mass ~148 g/mol), not the monomer (74 g/mol) (1 mark). Propan-1-ol forms only one H-bond per molecular interaction; breaking this single H-bond requires less energy (1 mark). Therefore, despite propanoic acid having a slightly higher molecular mass, the energy required to disrupt its dimer is far greater, giving it a 44°C higher boiling point than propan-1-ol (1 mark).

Q8 (6 marks) — sample:

Carboxylate vs alkoxide: When ethanoic acid loses H⁺, it forms the ethanoate ion (CH₃COO⁻). The negative charge is delocalised across both oxygen atoms by resonance: CH₃–C(=O)–O⁻ ↔ CH₃–C(–O⁻)=O — each oxygen carries approximately half a negative charge (2 marks). This resonance stabilisation makes the ethanoate ion a relatively weak base (less tendency to re-accept H⁺), so the equilibrium lies further toward ionisation — ethanoic acid is a stronger acid (pKa ~5) (1 mark). When ethanol loses H⁺, the ethoxide (CH₃CH₂O⁻) has the full negative charge localised on a single oxygen — no resonance stabilisation. This strong base readily re-accepts H⁺, so the equilibrium lies far left — ethanol is a very weak acid (pKa ~16) (1 mark).

Student claim evaluation: The student is correct (1 mark). Electronegative atoms like Cl attached to the alkyl chain exert an inductive effect — they withdraw electron density through the C–C bonds toward themselves, which partially stabilises the negative charge on the carboxylate oxygens beyond what resonance alone achieves (it reduces the electron density of the carboxyl group, making the O–H bond more polar and the conjugate base more stable). Chloroethanoic acid (CH₂ClCOOH) has pKa 2.86, significantly lower than ethanoic acid's 4.74, confirming it is a stronger acid (1 mark).

Revisit: Wine Turns to Vinegar

Now that you have studied carboxylic acids, revisit your Think First prediction. The reason ethanoic acid (118°C) has a dramatically higher boiling point than ethanol (78°C) — despite the acid being heavier — is dimerisation. The carboxyl group can simultaneously donate AND accept a H-bond, allowing two carboxylic acid molecules to lock together in a cyclic dimer via two H-bonds. Breaking this pair requires far more energy than breaking ethanol's single H-bond. This is something the simple –OH group in ethanol cannot do.

The acid strength difference (ethanoic acid pKa 4.74 vs ethanol pKa ~16) traces to the same structural feature: the adjacent C=O allows resonance in the carboxylate anion (charge on both O), making it a much weaker conjugate base than the ethoxide (charge on one O). One group — –COOH — gives carboxylic acids two major, interconnected advantages over alcohols.

Consolidation Game

Carboxylic Acids