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Temperature & Keq — Colourimetry

A chemist shines light through a deep red iron thiocyanate solution, reads an absorbance value, and — using Beer's Law and an ICE table — calculates Keq to four significant figures without ever measuring individual concentrations directly.

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Think First — Before You Read

📚 Know

  • Temperature is the only factor that changes the value of Keq
  • Endothermic reactions have Keq increase with temperature; exothermic reactions have Keq decrease
  • The Beer-Lambert law and calibration curve method for colourimetry

🔗 Understand

  • Why temperature affects Keq through collision theory and energy distribution
  • How colourimetry experimentally determines equilibrium concentrations
  • The qualitative connection between Gibbs free energy and Keq

✅ Can Do

  • Predict and justify the direction of Keq change with temperature
  • Calculate Keq from colourimetry data using a calibration curve
  • Use the van't Hoff equation qualitatively to compare Keq values at different temperatures

The equilibrium $\text{Fe}^{3+}(aq) + \text{SCN}^-(aq) \rightleftharpoons \text{FeSCN}^{2+}(aq)$ is exothermic in the forward direction (ΔH < 0). A student measures Keq at three temperatures: 25°C → Keq = 895; 35°C → Keq = 580; 45°C → Keq = 360.

Before reading on: (1) Do these values make sense given the sign of ΔH? (2) If the student measured at 15°C, would Keq be greater or less than 895? (3) What trend do you notice in how Keq changes per 10°C? Write your predictions.

Module 5 — Key Formulas: Lesson 13

Temperature effect on Keq: only temperature changes Keq
Exothermic forward (ΔH < 0): increase T → Keq decreases; decrease T → Keq increases
Endothermic forward (ΔH > 0): increase T → Keq increases; decrease T → Keq decreases
Beer-Lambert law: A = εlc  — A ∝ c for fixed ε and path length l
Calibration curve: absorbance → [FeSCN²⁺]eq → ICE table → Keq
Gibbs–Keq: ΔG° = −RT ln Keq  (qualitative + introductory quantitative in L14)
Large Keq → large negative ΔG° → forward reaction strongly spontaneous
Small Keq → large positive ΔG° → reverse reaction spontaneous
Keq = 1 → ΔG° = 0 → neither direction favoured under standard conditions

Misconceptions to Fix

Wrong: A large Keq means the reaction happens quickly.

Right: Keq indicates the equilibrium position — a large Keq means products are favoured at equilibrium. It says nothing about reaction rate. Rate depends on activation energy, temperature, and catalysts, not thermodynamic favourability. A reaction can have a huge Keq but be extremely slow.

Choose how you work — type your answers below or write in your book.

Key Terms — scan these before reading
Dynamic equilibriumA state where forward and reverse reaction rates are equal.
Le Chatelier's PrincipleA system at equilibrium shifts to minimise applied disturbances.
Equilibrium constant (Keq)The ratio of product to reactant concentrations at equilibrium.
Reaction quotient (Q)The ratio of product to reactant concentrations at any instant.
Closed systemA system where neither matter nor energy can escape to surroundings.
Reversible reactionA reaction that can proceed in both forward and reverse directions.
01

Card 1 — Temperature Is the Only Factor That Changes Keq

Every lesson in IQ2 and IQ3 has repeated that only temperature changes Keq — this card explains exactly why, at the thermodynamic level, and why no other factor can do the same.

Keq is related to the standard Gibbs free energy change: $\Delta G^\circ = -RT \ln K_{eq}$, which rearranges to $K_{eq} = e^{-\Delta G^\circ / RT}$.

Because $\Delta G^\circ = \Delta H^\circ - T\Delta S^\circ$, and this expression contains the term $T\Delta S^\circ$, ΔG° itself depends on temperature. As temperature changes, ΔG° changes — and therefore Keq changes.

No other factor — concentration, pressure, or catalyst — changes the thermodynamic energy landscape of the reaction (the stability of reactants vs products). They only change the system's current state (how far it currently is from equilibrium), not the thermodynamic destination.

Temperature increases
Keq decreases → shifts left
Keq increases → shifts right
Temperature decreases
Keq increases → shifts right
Keq decreases → shifts left
HSC Extended Response Wording: "Keq is determined by the thermodynamic stability of products relative to reactants (ΔG° = −RT ln Keq). Only temperature changes the thermodynamic energy landscape of the reaction — concentration, pressure, and catalyst changes affect the system's position relative to equilibrium but do not change the stability of reactants or products."
Common Error: "Increasing pressure makes more products form, so Keq must increase." Wrong — Keq is the ratio at equilibrium. Yes, more products form when pressure is increased (for reactions with fewer gas moles on the product side), but the denominator also changes. The ratio at the new equilibrium is the same Keq — satisfied with different absolute concentrations. The ratio is invariant at constant temperature.
TEMPERATURE CHANGE × ΔH SIGN → Keq EFFECT EXOTHERMIC fwd (ΔH < 0) treat as exo = heat is product ENDOTHERMIC fwd (ΔH > 0) treat as endo = heat is reactant INCREASE Temperature Keq DECREASES shift ← LEFT (less product) Keq INCREASES shift → RIGHT (more product) DECREASE Temperature Keq INCREASES shift → RIGHT (more product) Keq DECREASES shift ← LEFT (less product)

Temperature × ΔH matrix — Keq change and shift direction for all four combinations

Exam TipWhen explaining equilibrium shifts, always state the direction (left or right) and justify using Le Chatelier's Principle language — simply stating the direction alone will not earn full marks.
02

Card 2 — Temperature and Keq: Calculating and Interpreting Values

Temperature-dependent Keq data is one of the most frequently tested quantitative aspects of IQ3 — the calculation itself is simple, but interpreting what the changing Keq values tell you about ΔH requires careful reasoning.

From a table of Keq at different temperatures, you can determine:

  • Keq decreases as T increases → forward reaction is exothermic
  • Keq increases as T increases → forward reaction is endothermic

Think First data — iron thiocyanate (exothermic forward, ΔH < 0):

Keq
895
580
360
> 895
Interpretation
Higher Keq → more FeSCN²⁺ at equilibrium
↓ decreasing as T increases → exothermic forward ✓
↓ confirmed exothermic trend
Lower T → higher Keq for exothermic forward
Must Know (3 Required Points): In HSC questions providing a Keq-vs-temperature table, always explicitly state: (1) the direction of Keq change with temperature; (2) what this implies about the exo/endothermic nature of the forward reaction; (3) predictions for Keq outside the given temperature range. All three points are commonly assessed.
Beyond the Syllabus: The Van't Hoff equation formalises the temperature–Keq relationship: $\ln(K_2/K_1) = -\Delta H^\circ/R \times (1/T_2 - 1/T_1)$. This is beyond HSC scope but the qualitative principle — larger |ΔH°| means Keq is more sensitive to temperature — is useful context for understanding why some equilibria shift dramatically with temperature while others barely change.
03

Card 3 — Colourimetry: Measuring Keq Experimentally

Colourimetry converts the invisible (an equilibrium constant) into the visible (the intensity of a colour) — and by connecting absorbance to concentration, it turns a qualitative observation into a quantitative measurement.

The iron(III) thiocyanate equilibrium is ideal because FeSCN²⁺ is intensely red while Fe³⁺ and SCN⁻ are essentially colourless. The Beer-Lambert law states: for a fixed path length and molar absorptivity, absorbance (A) is proportional to the concentration of the absorbing species.

$$A = \varepsilon l c$$

where ε = molar absorptivity, l = path length (cm), c = concentration (mol/L).

Using a calibration curve (absorbance vs known [FeSCN²⁺] from standards), the equilibrium [FeSCN²⁺] in any sample can be read directly from the measured absorbance.

1
Prepare calibration standards — known [FeSCN²⁺] measured with colorimeter → plot A vs [FeSCN²⁺] → straight line through origin
2
Prepare equilibrium mixture from known initial [Fe³⁺] and [SCN⁻]
3
Measure absorbance of equilibrium mixture → use calibration curve to find [FeSCN²⁺]eq
4
Set up ICE table with known initial [Fe³⁺] and [SCN⁻] and measured [FeSCN²⁺]eq → calculate [Fe³⁺]eq and [SCN⁻]eq
5
Substitute all equilibrium concentrations into Keq expression → calculate Keq
Must Know (NESA Investigation): The colourimetry Keq experiment is a NESA-specified investigation. Describe the method using the 5 steps above and explain Beer-Lambert: "Absorbance is proportional to [FeSCN²⁺] — measuring absorbance allows [FeSCN²⁺]eq to be determined from the calibration curve, which is then used in the ICE table to find all equilibrium concentrations and calculate Keq."
Common Error: Describing colourimetry as "measuring the colour to find Keq" without explaining the quantitative connection. The key step is the calibration curve — it converts the absorbance reading (directly measurable) into a concentration (needed for the Keq calculation). Without the calibration step, the measurement gives no numerical Keq.
04

Card 4 — Calculating Keq from Colourimetry Data

The colourimetry calculation is an ICE table problem where one equilibrium concentration (the coloured product) is given directly by the absorbance measurement — exactly the Type 2 ICE problem from L10.

Experimental setup: Initial [Fe³⁺] = 1.00 × 10⁻³ mol/L, initial [SCN⁻] = 1.00 × 10⁻³ mol/L. Absorbance measured → calibration curve gives: [FeSCN²⁺]eq = 1.50 × 10⁻⁴ mol/L.

ICE Table: $\text{Fe}^{3+}(aq) + \text{SCN}^-(aq) \rightleftharpoons \text{FeSCN}^{2+}(aq)$

Initial (mol/L)

Fe³⁺: 1.00 × 10⁻³
SCN⁻: 1.00 × 10⁻³
FeSCN²⁺: 0

Change (mol/L)

Fe³⁺: −1.50 × 10⁻⁴
SCN⁻: −1.50 × 10⁻⁴
FeSCN²⁺: +1.50 × 10⁻⁴

Equilibrium (mol/L)

Fe³⁺: 8.50 × 10⁻⁴
SCN⁻: 8.50 × 10⁻⁴
FeSCN²⁺: 1.50 × 10⁻⁴

Keq calculation:

$$K_{eq} = \frac{[\text{FeSCN}^{2+}]}{[\text{Fe}^{3+}][\text{SCN}^-]} = \frac{1.50 \times 10^{-4}}{(8.50 \times 10^{-4})(8.50 \times 10^{-4})}$$

Denominator: $(8.50 \times 10^{-4})^2 = 7.225 \times 10^{-7}$

$$K_{eq} = \frac{1.50 \times 10^{-4}}{7.225 \times 10^{-7}} = 207.6 \approx 208 \checkmark$$

Must Know (Stoichiometry): In the Fe³⁺ + SCN⁻ ⇌ FeSCN²⁺ ICE table, the stoichiometric ratio is 1:1:1 — one mole of Fe³⁺ reacts with one mole of SCN⁻ to produce one mole of FeSCN²⁺. The Change row entries for Fe³⁺ and SCN⁻ are both equal (in magnitude) to the change in FeSCN²⁺. Never assume all ICE tables have equal changes — always check stoichiometric coefficients first.
Common Error: Calculating equilibrium [Fe³⁺] correctly but forgetting to apply the same change to [SCN⁻]. In this symmetric case (equal initial concentrations, 1:1:1 stoichiometry), [Fe³⁺]eq = [SCN⁻]eq. In asymmetric cases, the changes are equal in magnitude but the equilibrium concentrations will differ.
05

Card 5 — Gibbs Free Energy and Keq: The Qualitative Connection

The equation ΔG° = −RT ln Keq is the bridge between thermodynamics and equilibrium — it connects the spontaneity of a reaction (from Module 4) to the position of that reaction's equilibrium.

The relationship $\Delta G^\circ = -RT \ln K_{eq}$ encodes the following qualitative relationships:

Keq valueln KeqΔG°Interpretation
Large (>> 1) Large positive Large negative Products strongly favoured; forward reaction highly spontaneous
= 1 = 0 = 0 Neither direction favoured under standard conditions
Small (<< 1) Large negative Large positive Reactants strongly favoured; reverse reaction spontaneous

Examples:

  • $\text{H}_2(g) + \frac{1}{2}\text{O}_2(g) \rightarrow \text{H}_2\text{O}(g)$, Keq ≈ 10⁴⁰ → ΔG° = very large negative → water formation massively spontaneous.
  • $\text{N}_2(g) + \text{O}_2(g) \rightleftharpoons 2\text{NO}(g)$, Keq = 10⁻³⁰ → ΔG° = very large positive → NO formation massively non-spontaneous at 25°C.
HSC Scope: You need the qualitative relationship only for most questions: large Keq → negative ΔG° → forward reaction spontaneous; small Keq → positive ΔG° → forward reaction non-spontaneous; Keq = 1 → ΔG° = 0. The full quantitative calculation ΔG° = −RT ln Keq is introduced in L14.
Insight — Resolves a Module 4 Confusion: In M4 you learned ΔG < 0 means a reaction is spontaneous — but many spontaneous reactions don't go to completion. Resolution: ΔG° < 0 means the forward direction is spontaneous under standard conditions, but equilibrium is reached before completion if Keq is not extremely large. The system reaches minimum free energy at the equilibrium composition, not at complete conversion. ΔG = 0 at equilibrium (not ΔG°).
ΔG° = −RT ln Keq — The Bridge: Thermodynamics ↔ Equilibrium Keq scale: 10⁻³⁰ 10⁻¹⁰ 10⁰ = 1 10⁺¹⁰ 10⁺³⁰ ΔG° sign: very +ve +ve ≈ 0 −ve very −ve REACTANTS strongly favoured Reverse reaction spontaneous eg. N₂+O₂→2NO: Keq≈10⁻³⁰ Mixed — both present Neither strongly favoured eg. N₂+3H₂→2NH₃: Keq≈10⁶ PRODUCTS strongly favoured Forward reaction spontaneous eg. H₂+½O₂→H₂O: Keq≈10⁴⁰
06

Worked Examples

Example 1 — Interpreting Temperature-Dependent Keq Data Band 5

The following Keq values are measured for $\text{A}(g) + \text{B}(g) \rightleftharpoons 2\text{C}(g)$: at 300°C, Keq = 0.25; at 400°C, Keq = 1.10; at 500°C, Keq = 4.80. (a) Is the forward reaction exothermic or endothermic? (b) At 200°C, would Keq be greater or less than 0.25? (c) A chemist claims Keq = 4.80 at 500°C means the equilibrium "strongly favours products." Evaluate this claim.

Step 1 — Part (a): Determine ΔH Direction

Keq increases as temperature increases: 0.25 → 1.10 → 4.80. Increasing temperature shifts the equilibrium in the endothermic direction. Since Keq increases (more products) as T increases, higher temperature favours the forward reaction → the forward reaction is endothermic (ΔH > 0). Consistent with LCP: adding heat shifts toward endothermic direction (right), producing more C.

Step 2 — Part (b): Predict Keq at 200°C

For an endothermic forward reaction, decreasing T decreases Keq. At 200°C (lower than 300°C): Keq < 0.25. Equilibrium would favour reactants even more than at 300°C.

Step 3 — Part (c): Evaluate the Claim

Keq = 4.80. Is 4.80 >> 1? No — 4.80 is moderately greater than 1. "Strongly favours products" implies Keq >> 1 (e.g. 10³ or higher). Keq = 4.80 is better described as "products are moderately favoured" — significant concentrations of both reactants and products would be present at equilibrium.

Answer: (a) Endothermic forward — Keq increases with T. (b) Keq < 0.25 at 200°C. (c) Claim overstated — Keq = 4.80 is moderately > 1; products somewhat favoured but significant reactants remain. ✓

Example 2 — Full Colourimetry Keq Calculation Band 5–6

A student prepares an equilibrium mixture for $\text{Fe}^{3+}(aq) + \text{SCN}^-(aq) \rightleftharpoons \text{FeSCN}^{2+}(aq)$ with initial [Fe³⁺] = 2.00 × 10⁻³ mol/L and initial [SCN⁻] = 2.00 × 10⁻³ mol/L. After equilibrium, using the calibration curve: [FeSCN²⁺]eq = 4.80 × 10⁻⁴ mol/L. (a) Set up and complete the ICE table. (b) Calculate Keq. (c) Verify by substitution.

Step 1 — Part (a): ICE Table
Fe³⁺SCN⁻FeSCN²⁺
Initial (mol/L)2.00 × 10⁻³2.00 × 10⁻³0
Change (mol/L)−4.80 × 10⁻⁴−4.80 × 10⁻⁴+4.80 × 10⁻⁴
Equilibrium (mol/L)1.52 × 10⁻³1.52 × 10⁻³4.80 × 10⁻⁴

Equilibrium [Fe³⁺] = 2.00 × 10⁻³ − 4.80 × 10⁻⁴ = 1.52 × 10⁻³ mol/L (same for [SCN⁻] by symmetry).

Step 2 — Part (b): Calculate Keq

$$K_{eq} = \frac{4.80 \times 10^{-4}}{(1.52 \times 10^{-3})(1.52 \times 10^{-3})} = \frac{4.80 \times 10^{-4}}{2.3104 \times 10^{-6}} = 207.7 \approx \mathbf{208}$$

Step 3 — Part (c): Verify

$(1.52 \times 10^{-3})^2 = 2.3104 \times 10^{-6}$ ✓; $4.80 \times 10^{-4} / 2.3104 \times 10^{-6} = 207.7$ ✓

Answer: (a) ICE table as above. (b) Keq = 208 at this temperature. (c) Verified ✓. Keq >> 1 → products significantly favoured — consistent with the deep red colour of FeSCN²⁺ visible even at low initial concentrations.
Interactive — Temperature-Keq Colour Predictor
Revisit Your Thinking

For an exothermic reaction (ΔH < 0), increasing temperature decreases Keq because heat acts as a product. The data showed Keq dropping from 895 at 25°C to 580 at 35°C to 360 at 45°C, confirming the forward reaction is exothermic. At 15°C, Keq would be greater than 895. A colourimetric experiment measures [FeSCN²⁺] at equilibrium, and from this you can calculate Keq using the ICE table and the initial concentrations.

Revisit Your Initial Thinking

Look back at what you wrote in the Think First section. What has changed? What did you get right? What surprised you?

07

Practice Questions

Q1. The equilibrium $\text{CO}(g) + 3\text{H}_2(g) \rightleftharpoons \text{CH}_4(g) + \text{H}_2\text{O}(g)$ has Keq = 3.90 × 10⁶ at 300°C and Keq = 1.85 × 10⁻² at 800°C. Which correctly interprets this data?

A The forward reaction is endothermic — Keq decreases as temperature increases
B The forward reaction is exothermic — Keq decreases as temperature increases, consistent with equilibrium shifting left at higher temperature
C Temperature has decreased Keq, so increasing pressure would restore the original Keq
D The forward reaction is endothermic because Keq is large at 300°C

Q2. In a colourimetry experiment for $\text{Fe}^{3+} + \text{SCN}^- \rightleftharpoons \text{FeSCN}^{2+}$, a calibration curve is used to determine [FeSCN²⁺]eq from the measured absorbance. Why is the calibration curve necessary?

A To measure the temperature dependence of Keq at each wavelength
B To convert the absorbance reading (directly measurable) into a concentration (needed for the Keq calculation), using the Beer-Lambert relationship A ∝ c
C To correct for the colour of Fe³⁺ and SCN⁻ which interfere with the measurement
D To determine the wavelength at which FeSCN²⁺ absorbs light most strongly

Q3. For the equilibrium $2\text{NO}_2(g) \rightleftharpoons 2\text{NO}(g) + \text{O}_2(g)$, ΔG° = +70 kJ/mol at 298 K. Which statement is consistent with this value?

A Keq > 1; products are favoured at 298 K
B Keq < 1; reactants are favoured; ΔG° = −RT ln Keq gives a positive ΔG° when Keq < 1
C Keq = 1; ΔG° = 0 at equilibrium so Keq = 1
D Keq > 1; positive ΔG° means the reaction is exothermic and products are stable
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Lesson 13 complete — Temperature, Colourimetry & Gibbs